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RSC - CrystEngComm latest articles



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Copyright: Copyright (c) The Royal Society of Chemistry
 



Preparation, properties, formation mechanisms, and cytotoxicity of calcium oxalate monohydrate with various morphologies
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01912B, Paper
Xin-Yuan Sun, Chong-Yu Zhang, Poonam Bhadja, Jian-Ming Ouyang
Calcium oxalate monohydrate (COM) crystals with various morphologies, such as elliptical, hexagonal, peanut-like, spherical and flower-like structures with a size of about 10 [small mu ]m, were prepared through varying reactant concentration,...
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Facile Synthesis and Heteroepitaxial Growth Mechanism of Au@Cu Core-Shell Bimetallic Nanocubes Probed by First-Principles Studies
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01617D, Paper
Changshun Wang, Junlong Li, Yeke Lou, Caixia Kan, Yan Zhu, Xiaoqin Feng, Yuan Ni, Haiying Xu, Daning Shi, Xinyuan Wei
Bimetallic Au@Cu core-shell nanocrystals have been synthesized by a two-step seed-mediated growth method through controlled heteroepitaxial growth of Cu shells on Au nanorods serving as seeds. The final crystal structures...
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Influence of substituents on the acceptor properties of the amino groups in the diaminobenzene analogues

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01732D, Paper
Svitlana V. Shishkina, Irina S. Konovalova, Oleg. V. Shishkin, Alexander N. Boyko
The influence of substituents on the geometric parameters and acceptor properties of the amino group in the diaminobenzene analogues has been studied using quantum-chemical calculations and the study of crystal packing from the energetic viewpoint.
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A Non-Interpenetrated Cu-based MOF Constructed from a Rediscovered Tetrahedral Ligand
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01818E, Paper
Komal M Patil, Shane Telfer, Stephen Moratti, Omid T Qazvini, Lyall R Hanton
A systematic expansion of the well-known non-interpenetrated and robust MOF-11 was accomplished through a rediscovery of the ligand tetrakis(4-carboxyphenyl)adamantane (L). The combination of a rigid tetrahedral L and copper(II) paddle-wheel...
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Structure guided or structure guiding? Mixed carbon/hydrogen bonding in a bis-Schiff base of N-allyl isatin

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01697B, Communication
Majid Hussain, Antonio Bauza, Antonio Frontera, Kong Mun Lo, Muhammad Moazzam Naseer
A supramolecular motif listed as 'carbon bonded' or 'hydrogen bonded' may have the character of both. We highlight the hybrid character of the non-covalent interaction in a bis-Schiff base of N-allyl isatin by combining theory and experiment.
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An exploration into the amide-pseudo amide hydrogen bonding synthon between a new coformer with two primary amide groups and theophylline

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01666B, Paper
Datta Markad, Sanjay K. Mandal
Double the FUN! A rare amide-pseudo amide hydrogen bonding synthon has been established for the co-crystal between a new coformer with two primary amide groups and theophylline.
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The Impact of Vinylene Bridges and Side Chain Alkyl Groups on Solid State Structures of Tricyanovinyl-Substituted Thiophenes
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01574G, Paper
Phuong-Truc T Pham, MAMOUN BADER
This goal of this work is to examine the solid state structures of compounds that have been designed for increased conjugation and solubility, as these factors are important if these...
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Boric Acid Co-crystals in Guar Gelation
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01858D, Paper
Andrea Perrin, Melissa J. Goodwin, Osama Musa, Dimitrii S Yufit, Jonathan W Steed
A series of bis(pyrrolidone) and -caprolactam co-crystals of boric acid and 1,4-phenylenediboronic acid are reported. The high polarity of the lactam carbonyl group is highly complementary to the boronic acid...
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Structural aspects of partial solid solution formation: Two crystalline modifications of chiral derivative of 1,5-dihydro-2H-pyrrol-2-one under consideration
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01717K, Paper
Olga Lodochnikova, Liliya Kosolapova, Alina Saifina, Aidar Timergalievich Gubaidullin, Robert R. Fayzullin, Khamatgalimov Ayrat, Igor Litvinov, Almira Kurbangalieva
The purposeful change of crystallization conditions for rac-3-chloro-5-hydroxy-1-(4-methylbenzyl)-4-[(4-methylphenyl)sulfanyl]-1,5-dihydro-2H-pyrrol-2-one 1 leads to two different crystal modifications, namely a racemic compound in the triclinic space group P-1 with Z' = 1 ([small alpha]-1)...
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Cyclometallated Platinum(II) and Palladium(II) Complexes Containing 1,5-Diarylbiguanides: Synthesis, Characterisation and Hydrogen Bond-directed Assembly
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01805C, Paper
David McMorran, Aidan P McKay, Keith Gordon, Georgina E Shillito
Complexes of the type [M(ppy)(big)], (where M = Pt(II) and Pd(II), ppy is 2-phenylpyridine and big is a 1,5-diarylbiguanide) have been prepared and characterised in solution and in the solid...
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Tb(III)-functionalized a new layer-like Cd MOF as luminescent probe for highly selectively sensing Cr3+
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01795B, Paper
Yi Wang, Huan Yang, Gang Cheng, yunying Wu, Shaomin Lin
A new layer-like metal-organic framework {[Cd4(NDIC)4[round bullet, filled]5DMF[round bullet, filled]H2O]DMF}n (NDIC = 5-(5-Norbonene-2,3-dicarboximide)Isophthalic acid) has been synthesized with solvothermal[space]method. It was used as a parent framework to sensitize via encapsulating Tb3+ cations in Cd-MOF....
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Towards stable porous crystalline phases of molecular belts

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01679D, Communication
Marco Bernabei, Raul Perez-Soto, Ismael Gomez Garcia, Maciej Haranczyk
A chemical modification of a molecular belt (M1) renders the molecule (M2) into a stable supramolecular nanotube porous crystal.
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Hierarchically structured magnesium based oxides: synthesis strategies and applications in organic pollutant remediation

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01755C, Highlight
Lekha Sharma, Rita Kakkar
In this highlight, we review the design and formation of MgO based hierarchical structures and cover some selected examples on their applications in adsorption of organic contaminants.
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A novel 3D POMOF based on Wells-Dawson arsenomolybdates with excellent photocatalytic and lithium-ion battery performance

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01734K, Paper
Bo-Wen Cong, Zhan-Hua Su, Zhi-Feng Zhao, Bo Wang
A novel 3D POMOF based on Wells-Dawson arsenomolybdates exhibits fluorescence property and efficient and stable photocatalytic activity for MB and RhB under UV irradiation and has also been evaluated as the anode material for LIBs.
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Polymorphs of daidzein and intermolecular interaction effect on solution crystallization

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01716B, Paper
Lina Jia, Shijie Xu, Shiyuan Liu, Shichao Du, Songgu Wu, Junbo Gong
Polymorphs of DAID with enhanced dissolution rates were discovered and the intermolecular interaction effect on crystallization behavior was investigated.
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Solvent-Controlled Synthesis of Various Anderson-type Polyoxometalate-based Metal-Organic Complexes with Excellent Capacity for Chromatographic Separation of Dyes
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01092C, Paper
Xiuli Wang, ge song, Hongyan Lin, Xiang Wang, Guocheng Liu, Xing Rong
Abstract: By changing solvent systems, five new Anderson-type polyoxometalates (POMs)-based metal-organic complexes, namely, {(H2PCAP')2[CrMo6(OH)5O19]}[round bullet, filled]H2O (1), {Cu3(PCAP)2[CrMo6(OH)5O19](H2O)3(DMF)2}[round bullet, filled]4H2O[round bullet, filled]2HCHO (2), {Cu3(PCAP)2[CrMo6(OH)6O18]Cl(H2O)5}[round bullet, filled]10H2O (3), {Co3(PCAP)2[CrMo6(OH)5O19](H2O)6}[round bullet, filled]9H2O[round bullet, filled]HCHO (4), {Co3(HPCAP)2[CrMo6(OH)6O18]2(H2O)10}[round bullet, filled]7H2O[round bullet, filled]2CH3CH2OH (5) (HPCAP= 3-(2-pyridinecarboxylic acid amido)pyridine, PCAP'= 3-(pyridinecarboxylic acid)amido...
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Controllable synthesis of two CaO crystal generations: precursors' synthesis and formation mechanisms

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01561E, Paper
Liang Ma, Bosheng Zhao, Huihu Shi, Feng Sha, Chang Liu, Hong Du, Jianbin Zhang
In this study, novel rod-like and block-like CaO crystals were prepared after calcinating three types of CaCO3 precursors containing dumbbell-like, wheat spike-like and microsphere-like morphologies at 1000 [degree]C for 3 h.
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Highly tuneable proton-conducting coordination polymers derived from a sulfonate-based ligand

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01589E, Paper
Mei-Jie Wei, Jia-Qi Fu, Yi-Di Wang, Yi Zhang, Hong-Ying Zang, Kui-Zhan Shao, Yang-Guang Li, Zhong-Min Su
Three highly proton-conducting coordination compounds have been synthesized via the HCl steaming-assisted conversion approach by using multiple functional groups including the sulfonate group and the Cl- or HPO42- group.
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One-pot scalable synthesis of all-inorganic perovskite nanocrystals with tunable morphology, composition and photoluminescence

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01749A, Paper
Emmanuel Acheampong Tsiwah, Yanxi Ding, Zixiong Li, Zhiyong Zhao, Mingqing Wang, Chao Hu, Xiaoqing Liu, Chenghua Sun, Xiujian Zhao, Yi Xie
Tuning the morphology, composition and photoluminescence emission over almost the entire visible region of all-inorganic cesium lead halide nanocrystals by a general and facile one-pot synthetic approach.
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An uncommon 3D 3,3,4,8-c Cd(II) metal-organic framework for highly efficient luminescent sensing and organic dye adsorption: experimental and theoretical insight

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01638G, Paper
Lu Lu, Jian Wu, Jun Wang, Jian-Qiang Liu, Bao-Hong Li, Amita Singh, Abhinav Kumar, Stuart R. Batten
A stable 3D Cd(II) MOF used as chemosensor and adsorbent for dyes in wastewater, which exhibited excellent adsorption performance and selectivity.
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One-dimensional lead borate nanowhiskers for joint shielding of neutron and gamma radiations: controlled synthesis, microstructure, and performance evaluation
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01547J, Paper
You Wu, Quan-Ping Zhang, Dong Zhou, Li-Ping Liu, Chuan Yun Xu, Dui-Gong Xu, Yuanlin Zhou
Lead borate nanowhiskers have been successfully prepared by a facile low-temperature solvothermal method. The morphologies and crystal sizes of the lead borate nanowhiskers are controlled by adjusting the amount of...
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Preparation and crystal structures of charge-transfer complexes of acyclic host molecules bearing pyrogallol derivatives with paraquat
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01748K, Paper
Masatoshi Kawahata, Masahide Tominaga, Yumi Maekawa, Kentaro Yamaguchi
Adamantane-based molecules possessing two or three pyrogallol derivatives as acyclic host molecules were developed to examine their potential to form complexes with pyridinium-based dicationic compounds, which are well known as...
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Highly thermally stable heterogeneous catalysts: study of 0D and 3D porphyrinic MOFs
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01702B, Paper
Eder Amayuelas Lopez, Arkaitz Fidalgo-Marijuan, Begona Bazan, Miren Karmele Urtiaga, Gotzone Barandika, Maria Isabel Arriortua
Heterogeneous catalysts are a great bet for green chemistry in many industrial processes and, in the past decade, promising results have been achieved in order to improve the catalytic activity...
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Coordination polymer based perovskite device: matched energy levels and photocurrent enhancement in the absence or presence of methanol

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01682D, Paper
Sen Lv, Zhe Yuan Wang, Xu Gu, Chong Zhang, Yun Gong, Jian Hua Lin
A coordination polymer based perovskite device yielded much larger photocurrent density with or without methanol under visible light illumination, which is ascribed to their matched VBM/CBM energy levels.
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Epitaxial growth of single crystalline film scintillators based on the Pr3+ doped solid solution of Lu3Al5-xGaxO12 garnet

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01376K, Paper
V. Gorbenko, T. Zorenko, K. Paprocki, B. Machlovanyi, B. Mazalon, A. Fedorov, Ya. Zhydachevskyy, A. Suchocki, Yu. Zorenko
Scintillating screens based on single crystalline films of Lu3Al5-xGaxO12:Pr garnet have been developed by the LPE method onto YAG substrates using BaO based flux.
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Correction: pH-Triggered construction of NLO active CMOFs: change in supramolecular assembly, water clusters, helical architectures and their properties
CrystEngComm, 2017, 19,6720-6720
DOI: 10.1039/C7CE90157G, Correction
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Rajat Saha, Susobhan Biswas, Golam Mostafa
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Crystallisation temperature control of stoichiometry and selectivity in host-guest compounds
CrystEngComm, 2017, 19,6719-6719
DOI: 10.1039/C7CE90166F, Correction
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Nicole M. Sykes, Hong Su, Edwin Weber, Susan A. Bourne, Luigi R. Nassimbeni
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1D Cu@Ni nanorods anchored on 2D reduced graphene oxide with interfacial engineering to enhance microwave absorption properties

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CrystEngComm, 2017, 19,6579-6587
DOI: 10.1039/C7CE01439B, Paper
Biao Zhao, Luyang Liang, Jiushuai Deng, Zhongyi Bai, Junwei Liu, Xiaoqin Guo, Ka Gao, Wenhui Guo, Rui Zhang
In this work, one-dimensional core-shell Cu@Ni nanorods which were anchored on two dimensional reduced graphene oxide (rGO) heterostructures were successfully prepared by a simple co-reduction method.
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Significant improvement of multi-seed method of diamond synthesis by adjusting the lateral cooling water temperature

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CrystEngComm, 2017, 19,6681-6685
DOI: 10.1039/C7CE01685A, Paper
Yadong Li, Chunxiao Wang, Ning Chen, Liangchao Chen, Longsuo Guo, Xiaopeng Jia, Hong-an Ma
In this work, we use a multi-seed arrangement assembly with an annular carbon source to synthesize large single-crystals of diamond and investigate the influence of the external environment on the synthesis of diamonds.
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Atomic structure-dominated enhancement of acetone sensing for a ZnO nanoplate with highly exposed (0001) facet

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CrystEngComm, 2017, 19,6711-6718
DOI: 10.1039/C7CE01759F, Paper
Mingjing Wang, Zhurui Shen, Yalu Chen, Ying Zhang, Huiming Ji
Multilayer-assembled ZnO nanoplates predominantly exposed (0001) polar facet, but displayed best gas sensing performance with very few oxygen vacancies, due to its special atomic structure.
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Pseudopolymorphism based on 1D metallacyclic chains constructed from an angular zwitterionic ditopic diacid organic linker

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CrystEngComm, 2017, 19,6686-6693
DOI: 10.1039/C7CE01568B, Paper
Yong-Qing Huang, Zong-Ge Li, Huai-Ying Chen, Hai-Di Cheng, Yang Wang, Yong-He Ren, Yue Zhao, Li Liu
Two pseudopolymorphs based on one dimensional metallacyclic chains display crystalline-form-dependent optical properties.
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Effect of precursor concentration on size evolution of iron oxide nanoparticles

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CrystEngComm, 2017, 19,6694-6702
DOI: 10.1039/C7CE01406F, Paper
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Hamed Sharifi Dehsari, Anielen Halda Ribeiro, Bora Ersoz, Wolfgang Tremel, Gerhard Jakob, Kamal Asadi
Changing the precursor concentration to tune the iron-oxide nanoparticle size alters the surfactant/precursor ratio and leads to the observation of two size regimes.
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Rapid augmentation of vertically aligned MoO3 nanorods via microwave irradiation

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CrystEngComm, 2017, 19,6568-6572
DOI: 10.1039/C7CE01531C, Communication
Kaushalendra K. Singh, Vivek Ramakrishnan, Ramya Prabhu B., Neena S. John
Microwave assisted rapid growth of vertically aligned hexagonal MoO3 nanorods on rigid substrates and its inter-conversion to orthorhombic form.
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Nanoparticles in [small beta]-tricalcium phosphate substrate enhance modulation of structure and composition of an octacalcium phosphate grown layer

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CrystEngComm, 2017, 19,6660-6672
DOI: 10.1039/C7CE01563A, Paper
Kazuo Onuma, Mayumi Iijima
Nanoparticles in the [small beta]-TCP substrate enhance structural modulation of an OCP grown layer.
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Magnetic properties and luminescence sensing of five coordination polymers based on a rigid terphenyl-tetracarboxylic acid

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CrystEngComm, 2017, 19,6651-6659
DOI: 10.1039/C7CE01510K, Paper
Ling-Ling Gao, Qian-Nan Zhao, Miao-Miao Li, Li-Ming Fan, Xiao-Yan Niu, Xiao-Qing Wang, Tuo-Ping Hu
Five terphenyl-tetracarboxylic acid based on CPs with variable-temperature magnetic susceptibilities and luminescence sensing of small organic molecules.
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How explosive TNP interacts with a small tritopic receptor: a combined crystallographic and thermodynamic approach

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CrystEngComm, 2017, 19,6703-6710
DOI: 10.1039/C7CE01494E, Paper
Pritam Ghosh, Suparna Paul, Priyabrata Banerjee
The interaction of explosive and pollutant TNP with the host receptor has been thoroughly explained and characterized by SCXRD and thermodynamic parameters.
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A Zn(II) complex with large channels based on 3[prime or minute]-nitro-biphenyl-3,5,4[prime or minute]-tricarboxylic acid: synthesis, crystal structure, fluorescence sensing of ATP, ADP, GTP, and UTP in aqueous solution and drug delivery

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CrystEngComm, 2017, 19,6673-6680
DOI: 10.1039/C7CE01618B, Paper
De-chun Zhang, Xia Li
A 3D Zn(II)-MOF with large cubic channels was synthesized. It showed fluorescence sensing of ATP, ADP, GTP, and UTP. Furthermore, it exhibited a remarkable capacity for and controlled release of 5-fluorouracil.
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Syntheses, structural diversity, magnetic properties and dye absorption of various Co(II) MOFs based on a semi-flexible 4-(3,5-dicarboxylatobenzyloxy)benzoic acid

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CrystEngComm, 2017, 19,6630-6643
DOI: 10.1039/C7CE01229B, Paper
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Xiang-min Meng, Lian-sheng Cui, Xin-ping Wang, Xiao-yin Zhang, Xia Zhang, Shuang-yu Bi
Various polymeric structures of MOFs 1-5.
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Micro-sectoriality in hydrothermally grown ruby crystals: the internal structure of the boundaries of the growth sectors

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CrystEngComm, 2017, 19,6594-6601
DOI: 10.1039/C7CE01520H, Paper
Victor G. Thomas, Nina Daneu, Aleksander Recnik, Rudolf I. Mashkovtsev, Goran Drazic, Sandra Drev, Sergey P. Demin, Pavel N. Gavryushkin, Dmitry A. Fursenko
This study explores the fine structural details of the boundaries between the growth micro-sectors in a ruby crystal grown hydrothermally on a nonsingularly oriented (01[1 with combining macron][2 with combining macron]) seed.
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Simple coordination complex-derived Ni NP anchored N-doped porous carbons with high performance for reduction of nitroarenes

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CrystEngComm, 2017, 19,6612-6619
DOI: 10.1039/C7CE01571B, Paper
Dan Xu, Ying Pan, Liangkui Zhu, Yusran Yusran, Daliang Zhang, Qianrong Fang, Ming Xue, Shilun Qiu
N-doped hierarchical porous carbons anchored with nickel nanoparticles were prepared by using the simple coordination complex Ni(dmg)2 as a precursor.
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Alkali earth MOx (x = 6, 7, 9, 12) polyhedra tuned cadmium selenites with different dimensions and diverse SeO32- coordinations

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CrystEngComm, 2017, 19,6644-6650
DOI: 10.1039/C7CE01461A, Paper
Ying-Jie Jia, Yi-Gang Chen, Xiao-Ni Yao, Xian-Ming Zhang
Alkali earth cation-tuned framework of cadmium selenites resulting in evolvement of the structures from high dimension to low dimension.
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Hierarchical architecture of CuInS2 microsphere thin films: altering laterally aligned crystallographic plane growth by Cd and V doping

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CrystEngComm, 2017, 19,6602-6611
DOI: 10.1039/C7CE01293D, Paper
Logu Thirumalaisamy, Ramesh Raliya, Shalinee Kavadiya, Soundarrajan Palanivel, Kunjithapatham Sethuraman, Pratim Biswas
Nano-flakes of self-assembled porous pristine and cadmium (Cd) and vanadium (V) doped copper indium disulphide (CuInS2 (CIS)) microspheres are synthesized.
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Size-controlled synthesis of Au nanorings on Pd ultrathin nanoplates as efficient catalysts for hydrogenation

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CrystEngComm, 2017, 19,6588-6593
DOI: 10.1039/C7CE01350G, Paper
Yu Han, Wenxing Wang, Penglin Jiang, Yucong Yan, Hui Zhang, Deren Yang
Small Au nanorings were synthesized by a seed-mediated growth on Pd nanoplates in the presence of Ag+ ions and exhibited substantially enhanced catalytic activities for hydrogenation.
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Oxyfluoride glass-ceramic fibers doped with Nd3+: structural and optical characterization

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CrystEngComm, 2017, 19,6620-6629
DOI: 10.1039/C7CE01380A, Paper
G. Gorni, R. Balda, J. Fernandez, I. Iparraguirre, J. J. Velazquez, Y. Castro, L. Pascual, G. Chen, M. Sundararajan, M. J. Pascual, A. Duran
Selective excitation in an oxyfluoride glass-ceramic optical fiber containing LaF3 nanocrystals doped with Nd3+.
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Selective crystallisation of carbamazepine polymorphs on surfaces with differing properties

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CrystEngComm, 2017, 19,6573-6578
DOI: 10.1039/C7CE01317E, Paper
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Huaiyu Yang, Cai L. Song, Ying X. S. Lim, Wenqian Chen, Jerry Y. Y. Heng
Surface-induced nucleation of carbamazepine (CBZ) in ethanol was investigated with different surface materials: glass, polytetrafluoroethylene (PTFE) and tin.
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Luminescent sulfonate coordination polymers: synthesis, structural analysis and selective sensing of nitroaromatic compounds

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01453H, Paper
Neetu Singh, Udai P. Singh, Ray J. Butcher
Enhanced fluorescence intensity of sulfonate coordination polymers on addition of picric acid.
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In-situ High Pressure Study of an Elastic Crystal by FTIR Spectroscopy
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01664F, Communication
Manish Kumar Mishra, Pallavi Prasanna Ghalsasi, M N Deo, Himal Bhatt, Himanshu Poswal, Soumyajit Ghosh, Somnath Ganguly
We performed an in-situ high pressure FTIR spectroscopic study on 2,3-dichlorobenzylidine-4-bromoaniline (DBA) crystal at pressures ranging from ambient pressure to 13.8 GPa at room temperature. The variations in the stretching...
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Metal-Organic Frameworks Based on Halogen-bridged Dinuclear-Cu-nodes as Promising Materials for High Performance Supercapacitor Electrodes
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01840A, Paper
bao li, xin xiong, liuyin zhou, Wenjie Cao, Fan Yu, Jiyuan Liang, Yazheng Wang, Si-Qian Hu
Two halogen-bridged di-nuclear Cu-based 3D porous Metal-Organic Frameworks (MOFs), {[Cu2Cl(OH)(L)2]∙(CH3OH)4}n (1) and {[Cu2Br(OH)(L)2]∙(CH3OH)4}n (2) , have been obtained via solvothermal methods with the bi-functional ligand (HL = 4,2[prime or minute]:6[prime or minute],4[double prime]-terpyridine-4[prime or minute]-carboxylic acid). These...
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Influence of mole-ratio on the coordination behaviour of a ditopic N2O2S2-macrocycle: endo/exocyclic silver(I) coordination polymer exhibiting desolvation-induced SCSC transformation
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01540B, Paper
Sujin Seo, Eunji Lee, Huiyeong Ju, Seulgi Kim, In-Hyeok Park, Jong Hwa Jung, Shim Sung Lee
Mole-ratio dependent formations of the macrocyclic silver(I) complexes with different coordination modes and topologies are reported. When one equivalent of AgPF6 was reacted with an N2O2S2-macrocycle (L), a typical endocyclic...
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Morphology control of layered Bi11Fe2.8Co0.2Ti6O33 microcrystals: critical role of NaOH concentration and citric acid

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01622K, Paper
Zhiang Li, Tong Chen, Jifang Chen, Dejuan Sun, Liu Liu, Min Liu, Yalin Lu
Morphology control of layered Bi11Fe2.8Co0.2Ti6O33 microcrystals: critical role of NaOH concentration and citric acid.
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Pre-design and synthesis of a five-fold interpenetrated pcu-type porous coordination polymer and its CO2/CO separation

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01649B, Communication
Haifei Cao, Suna Wang, Yang Wang, HongLiang Lyu, Rajamani Krishna, Zhiyong Lu, Jingui Duan, Wanqin Jin
The first five-fold interpenetrated PCP with pcu topology and high porosity was rationally designed and prepared, which showed high separation potential of CO2/CO mixtures.
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Solubility and in vitro drug permeation behavior of ethenzamide cocrystals regulated in physiological pH environments

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01626C, Paper
Rajiv Khatioda, Basanta Saikia, Pranab Jyoti Das, Bipul Sarma
Drug release behavior of few ethenzamide cocrystals was investigated at different pH buffers. Change in lipophilic behavior and conformational adjustment of drug along with supramolecular synthons were probed for their improved drug efficacy.
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Co-Co and Co-Fe Cyano-bridged Pentanuclear Clusters Based on Methylpyrazinyl-Diamine Tetradentate Ligand: Spin Crossover and Metal Substitution Effects
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01826F, Communication
Bin Fei, Jian Zhou, Zheng Yan, Sergii I. Shylin, Vadim Ksenofontov, Il'ya A. Gural'skiy, Xin Bao
A pentanuclear CoII-CoIII cluster complex has been developed in a solvothermal synthesis. Its highly stable metal-mixed iron-cobalt derivatives display robust spin crossover (T1/2 = 268 K) controlled by the degree...
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Control of interfacial reactions for growth of high-quality AlN epitaxial films on Cu(111) substrates
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01803G, Paper
Wenliang Wang, Yulin Zheng, Yuan Li, Xiaochan Li, Liegen Huang, Zhuoran Li, Zhenya Lu, Guoqiang Li
High-quality AlN epitaxial films have been epitaxially grown on Cu(111) substrates by pulsed laser deposition (PLD) through effectively controlling the interfacial reactions between AlN epitaxial films and Cu substrates. The...
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A Stage-by-Stage Phase-induction and Nucleation of Black Phosphorus from Red Phosphorus Under Low-pressure Mineralization
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01492A, Paper
Zhiyan Chen, ya-bo Zhu, Jia Lei, Wanying Liu, Yunke Xu, Peizhong Feng
In the preparation of black Phosphorene (BP) by means of low-pressure mineralization, the complex temperature program makes its synthesis mechanism complicated and confusing. Herein, orthorhombic BP crystal was successfully synthesized...
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Facile synthesis of 3D flower-like Cu2-xSe nanostructures via sacrificing template method and the excellent antibacterial activities
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01750B, Paper
Lianjie Zhu, Fubo Gao, Pengzhao Lv, Yan Zeng, Wenwen Wang, Wenjun Zheng
Three-dimensional (3D) flower-like Cu2-xSe film with hexagonal nanosheet hierarchical structure has been synthesized for the first time from a 3D flower-like CuO film precursor through a facile sacrificing template method...
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Control of chirality and catenation in cobalt and cadmium camphorate coordination complexes

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01712J, Paper
Jack J. Przybyla, Robert L. LaDuca
Five cobalt or cadmium camphorate coordination polymers with various flexible-tether dipyridylamide ligands were structurally characterized. {[Co2(D-cam)2(pdn)][middle dot]2H2O}n (3, pdn = N,N[prime or minute]-(propane-1,3-diyl)dinicotinamide) has a self-penetrated 446810 mab network. {[Cd2(D-cam)2(pdn)][middle dot]H2O}n (4) shows a new 3,7-connected 3D network. The cadmium complexes were assayed for luminescent and nitrobenzene detection properties.
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Controllable seeded flux growth and optoelectronic properties of bulk o-SiP crystals

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01676J, Paper
Chunlong Li, Shanpeng Wang, Xixia Zhang, Ning Jia, Tongtong Yu, Min Zhu, Duo Liu, Xutang Tao
Seeded flux growth of bulk o-SiP single crystals with a layered structure, clear photo-switching behavior and relatively fast response.
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Self-reversible thermofluorochromism of D-A-D triphenylamine derivatives and the effect of molecular conformation and packing

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01538K, Paper
Anu Kundu, Subramanian Karthikeyan, Dohyun Moon, Savarimuthu Philip Anthony
Triphenylamine based donor-acceptor-donor compounds exhibited conformation and packing dependent solid state fluorescence and self-reversible thermofluorochromism.
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A hierarchically structured anatase-titania/indium-tin-oxide nanocomposite as an anodic material for lithium-ion batteries

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE00903H, Paper
Yan Luo, Yiming Zhang, Jianguo Huang
A nanotubular titania/ITO nanocomposite is synthesized, exhibiting enhanced electrochemical performance as an anodic material for lithium-ion batteries.
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Selective MeCN/EtCN sorption and preferential inclusion of substituted benzenes in a cage structure with arylsulfonamide-armed anthraquinones

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01752A, Paper
Takashi Takeda, Shin-ichiro Noro, Takayoshi Nakamura, Yasutaka Suzuki, Jun Kawamata, Tomoyuki Akutagawa
The titled compounds 1,4 formed low-dimensional crystal structures with selective sorption/inclusion properties.
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Separation of C2/C1 hydrocarbons through a gate-opening effect in a microporous metal-organic framework

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01766A, Paper
Rong-Guang Lin, Libo Li, Rui-Biao Lin, Hadi Arman, Banglin Chen
Here we report highly selective C2 separation from methane in a porous metal-organic framework.
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Residual stress analysis of 4H-SiC crystals obtained by a top-seeded solution growth method

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01641G, Communication
Yeong-Jae Yu, Dae-Seop Byeon, Yun-Ji Shin, Su-Hun Choi, Myung-Hyun Lee, Won-Jae Lee, Seong-Min Jeong
The top-seeded solution growth (TSSG) method is an alternative technique for growing SiC which can reduce the defect levels in the crystal.
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Structures and phase transitions in neat 4,4[prime or minute]-di-tert-butyl-2,2[prime or minute]-bipyridyl and in its molecular complexes with either bromanilic or iodanilic acid

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01481C, Paper
M. Rok, P. Szklarz, M. Moskwa, M. Kijewska, J. Baran, G. Bator, W. Medycki, M. Zamponi
Using the DSC method, structural phase transitions (PTs) have been found at 165 and 219 K for 4,4[prime or minute]-di-tert-butyl-2,2[prime or minute]-bipyridyl (dtBBP), whereas for its complex with iodanilic acid (dtBBP[middle dot]IA) PT is found at 331 K.
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Ternary Pt-Pd-Ag alloy nanoflowers for oxygen reduction reaction electrocatalysis

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01721A, Paper
Aleksei Chalgin, Fenglei Shi, Fan Li, Qian Xiang, Wenlong Chen, Chengyi Song, Peng Tao, Wen Shang, Tao Deng, Jianbo Wu
Elemental composition, dimensionality and morphology are the main factors that influence the catalytic activity and stability of platinum-based and noble metal alloy nanocatalysts.
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Molecular dynamics simulations of aqueous glycine solutions
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01271C, Paper
Yuriy Geniyevich Bushuev, Svetlana Vladimirovna Davletbaeva, Oscar Koifman
Simulations of glycine aqueous solutions have been carried out to study the effect of increasing solute concentration on the aggregation of glycine zwitterions. The AMBER force field, coupled with three...
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Developing a Wattecs Parallel Autoclave System Synthesis Technique for Tailoring Surface Compositions and Valence States of Pt-Fe Alloys to Realize Bifunctional Electrocatalysis
CrystEngComm, 2017, Accepted Manuscript
DOI: 10.1039/C7CE01612C, Paper
Guangran Xu, Jiayin Liu, Baocang Liu, Xia Gong, Shasha Wang, Qin Wang, Jun Zhang
The development of bifunctional electrocatalysts for both methanol oxidation reaction (MOR) on the anode and oxygen reduction reaction (ORR) on the cathode is urgently demanded for promoting the electrochemical energy...
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Hexameric assembly of 5,17-di-substituted calix[4]arene in the solid state

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01515A, Paper
Yutaro Yamasaki, Ryo Sekiya, Takeharu Haino
Chiral 5,17-difunctionalized-25,26,27,28-tetrapropyloxycalix[4]arene possessing (S)-mandelamide arms ((S,S)-1) afforded cocrystals (S,S)-1[middle dot](solvent) (solvent = MeOH, EtOH, 1-PrOH, 2-PrOH, and CH3CN). Four of the five cocrystals contain unusual hexameric assembly of the calix[4]arene host.
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Novel meso-substituted trans-A2B2 porphyrins: synthesis and structure of their metal-mediated supramolecular assemblies

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01642E, Paper
Soumyabrata Goswami, Bharat Kumar Tripuramallu, Israel Goldberg
Five novel trans-A2B2 porphyrins and their corresponding coordination polymers with transition metals have been synthesized. Absorption and emission studies and structural investigations define the coordination patterns of these compounds in the solid state.
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Deformation-induced structure evolution of poly(butylene terephthalate)/poly(carbonate) blends during uniaxial stretching

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01465A, Paper
Wenyang Zhang, Jingqing Li, Yingrui Shang, Hongfei Li, Shichun Jiang, Lijia An
Phase separation occurs during deformation for all the PBT/PC samples. At large strains, microfibril slippage plays a leading role in the macroscopic strain.
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Architecture of packing in molecular crystals

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01701D, Paper
W. D. S. Motherwell
Molecular coordination shells have been used to classify crystal structures into similarity groups.
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Salts of 4-aminobutyric acid and 6-aminohexanoic acid behaving as molecular Velcro

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01597F, Paper
M. Rademeyer, B. van der Westhuizen
The structural diversity observed in a family of carboxyalkylammonium halide- and oxo-salts is investigated employing crystal engineering principles.
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Facet-selective interface design of a BiOI(110)/Br-Bi2O2CO3(110) p-n heterojunction photocatalyst

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01601H, Paper
Yin Peng, Ting Liu, Jian Xu, Ke Ke Wang, Yan Ge Mao
A BiOI(110)/Br-BOC(110) p-n heterostructure photocatalyst with a high interface quality was designed and synthesized by facet-dependent selective adsorption.
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Type I vs. quasi-type II modulation in CdSe@CdS tetrapods: ramifications for noble metal tipping

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CrystEngComm, 2017, 19,6443-6453
DOI: 10.1039/C7CE01558E, Paper
Nicholas G. Pavlopoulos, Jeffrey T. Dubose, Yawei Liu, Xing Huang, Nicola Pinna, Marc-Georg Willinger, Tianquan Lian, Kookheon Char, Jeffrey Pyun
We report on noble metal tipping of heterostructured nanocrystals (NCs) of CdSe@CdS tetrapods (TPs) as a chemical reaction to manifest energetic differences between type I and quasi-type II heterojunctions.
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Characterization of the three-dimensional residual stress distribution in SiC bulk crystals by neutron diffraction

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CrystEngComm, 2017, 19,6527-6532
DOI: 10.1039/C7CE01552F, Paper
Xuejian Xie, Xiaobo Hu, Xiufang Chen, Fafu Liu, Xianglong Yang, Xiangang Xu, Hong Wang, Jian Li, Peng Yu, Ruiqi Wang
The neutron diffraction method was adopted to study the three-dimensional residual stress distribution in SiC bulk crystals for the first time.
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Study of three solvates of sulfamethazine

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CrystEngComm, 2017, 19,6481-6488
DOI: 10.1039/C7CE01610G, Paper
Dipali Ahuja, Pauric Bannigan, Ake C. Rasmuson
Three solvates for sulfamethazine (SMT) are reported. The solvent interacts with SMT in a strong hydrogen bonding network imparting stability to the solvate structure.
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Controlled synthesis of one-dimensional BiOBr with exposed (110) facets and enhanced photocatalytic activity

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CrystEngComm, 2017, 19,6473-6480
DOI: 10.1039/C7CE01452J, Paper
Yin Peng, Jian Xu, Ting Liu, Yan-ge Mao
One-dimensional (1D) rod-like BiOBr with exposed (110) facets was synthesized using glucose as a capping agent and structure-directing agent. The BiOBr with exposed (110) facets exhibits outstanding photocatalytic activity for degrading MO dyes at high concentrations under solar light irradiation.
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Rapid synthesis of hierarchical, flower-like Ag microstructures with a gemini surfactant as a directing agent for SERS applications

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CrystEngComm, 2017, 19,6547-6555
DOI: 10.1039/C7CE01573A, Paper
Yan Xia, Zhinong Gao, Xueming Liao, Chenchen Pan, Yingfang Zhang, Xuesong Feng
Various hierarchical Ag microstructures, including sensitive SERS substrate flower-like structures, can be designed and rapidly synthesized under different conditions.
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Crystallization-induced reversible fluorescence switching of alkyl chain length dependent thermally stable supercooled organic fluorescent liquids

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CrystEngComm, 2017, 19,6489-6497
DOI: 10.1039/C7CE01650F, Paper
P. S. Hariharan, Dohyun Moon, Savarimuthu Philip Anthony
Triphenylamine fluorophore-produced alkyl chain length dependent stable fluorescent liquids and their crystallization-induced reversible fluorescence switching.
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Emerging La2O2CN2 matrix with controllable 3D morphology for photoluminescence applications

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CrystEngComm, 2017, 19,6498-6505
DOI: 10.1039/C7CE01418J, Paper
Huayu Bai, Yan Song, Dan Li, Qianli Ma, Xiangting Dong, Wensheng Yu, Ying Yang, Hui Yu, Jinxian Wang, Guixia Liu
Shape-controlled La2O2CN2 microstructures are synthesized and are used as hosts for doping with various RE3+ to realize different colored emissions.
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Facile solution combustion synthesis of MoO2 nanoparticles as efficient photocatalysts

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CrystEngComm, 2017, 19,6516-6526
DOI: 10.1039/C7CE01611E, Paper
Siyong Gu, Mingli Qin, Houan Zhang, Jidong Ma, Haoyang Wu, Xuanhui Qu
Efficient foam-like MoO2 photocatalysts assembled from 20-30 nm nanoparticles were one-step fabricated by a solution combustion synthesis method.
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Synthesis of novel hierarchical SiC-SiO2 heterostructures via a catalyst free method

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CrystEngComm, 2017, 19,6540-6546
DOI: 10.1039/C7CE01182B, Paper
Jixiang Dai, Jianjun Sha, Zhaofu Zhang, Junqi Shao, Yufei Zu, Mingkai Lei
Novel hierarchical SiC-SiO2 heterostructures were synthesized on a graphite paper substrate via a catalyst free method.
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Nucleation of octahedral titanate crystals using waste anodic electrolyte from the anodization of TiO2 nanotubes

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CrystEngComm, 2017, 19,6406-6411
DOI: 10.1039/C7CE01549F, Communication
Kar Chun Lee, Srimala Sreekantan, Zainal Arifin Ahmad, Khairul Arifah Saharudin, Mustaffa Ali Azhar Taib
Anodization conducted in ethylene glycol with H2O2 produces nanotube arrays. Octahedral crystals were extracted from the electrolyte waste for chemical recycling.
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Synthesis of variously shaped magnetic FeCo nanoparticles and the growth mechanism of FeCo nanocubes

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CrystEngComm, 2017, 19,6506-6515
DOI: 10.1039/C7CE01353A, Paper
Jie Yuan, Cai-Fu Li, Zhi-Quan Liu, Di Wu, Lihua Cao
TEM characterization of FeCo nanosheets and FeCo cubes.
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A 3D luminescent Zn(II) MOF for the detection of high explosives and the degradation of organic dyes: an experimental and computational study

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CrystEngComm, 2017, 19,6464-6472
DOI: 10.1039/C7CE01341H, Paper
Jun-Cheng Jin, Jian Wu, Yong-Xiang He, Bao-Hong Li, Jian-Qiang Liu, Rajendra Prasad, Abhinav Kumar, Stuart R. Batten
A 3D uncommon porous MOF 1 with a 4-c lonsdaleite (lon) topology based on binuclear Zn clusters behaves as a fluorescent chemosensor and a photocatalyst.
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Tuning the structure and Zn(II) sensing of lanthanide complexes with two phenylimidazophenanthrolines by acetonitrile hydrolysis

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CrystEngComm, 2017, 19,6533-6539
DOI: 10.1039/C7CE01576C, Paper
Xia Zhou, Jun-Ling Peng, Cai-Ying Wen, Ze-Yu Liu, Xing-Hao Wang, Jian-Zhong Wu, Yong-Cong Ou
1D/0D lanthanide complexes of phenylimidazophenanthrolines were constructed via hydrolysis of acetonitrile, and 0-Eu shows prompt photoemission response to Zn2+.
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Shape tuneable synthesis of perovskite structured rare-earth chromites RECrO3via a mild hydrothermal method

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CrystEngComm, 2017, 19,6436-6442
DOI: 10.1039/C7CE01555K, Paper
Shan Wang, Xiaofeng Wu, Long Yuan, Chenyang Zhang, Dayong Lu
Controllable synthesis of perovskite structured oxides with well-defined facets is a challenging but important route for crystal shape and facet dependent applications.
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V2O5 nanobelt arrays with controllable morphologies for enhanced performance supercapacitors

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CrystEngComm, 2017, 19,6412-6424
DOI: 10.1039/C7CE01444A, Paper
Jiahe Xu, Feng Zheng, Hanqin Gong, Lai Chen, Jiaheng Xie, Pengfei Hu, Yang Li, Yu Gong, Qiang Zhen
Controllable preparation of V2O5 nanobelt arrays as binder-free supercapacitive electrode materials and their charge-discharge mechanism.
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Novel amine templated three-dimensional zinc-organophosphonates with variable pore-openings

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CrystEngComm, 2017, 19,6425-6435
DOI: 10.1039/C7CE00994A, Paper
Avijit Kumar Paul, Rajendiran Kanagaraj, Ajay Kumar Jana, Pradip K. Maji
Amine templated three-dimensional zinc-organophosphates with different ring sizes have been obtained by varying the organic amine molecules. The figure shows the various net structures obtained during the study.
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Growth mechanism and electrochemical properties of hierarchical hollow SnO2 microspheres with a "chestnut" morphology

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CrystEngComm, 2017, 19,6454-6463
DOI: 10.1039/C7CE01288H, Paper
Huating Hu, Liming Wu, Paul Gebhardt, Xiaofei Zhang, Alexey Cherevan, Birgit Gerke, Rainer Pottgen, Andrea Balducci, Stefano Passerini, Dominik Eder
This work provides an in-depth study on the growth, crystallization and performance of hollow SnO2 spheres for Li-ion/Na-ion batteries.
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Open network structures from 2D hydrogen bonded networks: diaminotriazyl tetraoxapentacenes

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CrystEngComm, 2017, 19,6401-6405
DOI: 10.1039/C7CE01247K, Communication
Kenneth E. Maly, William Buck, Louise N. Dawe
Crystals of 1 show two-dimensional hydrogen-bonded sheets that are prevented from packing closely by the large core, resulting in open network structures.
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Charge directed assembly of CdTe/CdS nanoparticles inside monocrystalline KH2PO4

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01688C, Paper
D. Vorontsov, S. Filonenko, A. Kanak, G. Okrepka, Y. Khalavka
The synthesis of aqueous CdTe/CdS quantum dots (QDs) embedded in potassium dihydrogen phosphate KH2PO4 (KDP) is demonstrated.
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In situ synchrotron X-ray diffraction study of coherently embedded silver nanostructure growth in silicon

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01441D, Paper
Puspendu Guha, Raghavendra Rao Juluri, Anjan Bhukta, Arnab Ghosh, Santanu Maiti, Arpan Bhattacharyya, Velaga Srihari, Parlapalli V. Satyam
We report on the in situ growth of coherently embedded Ag nanostructures using real time temperature dependent synchrotron X-ray diffraction (XRD) measurements.
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CO2 adsorption and separation in covalent organic frameworks with interlayer slipping

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01647F, Paper
Abhishek Sharma, Ateeque Malani, Nikhil V. Medhekar, Ravichandar Babarao
In layered COFs, slipping results in non-monotonous variation in CO2 adsorption and higher uptakes were found near a slipping distance of 10 A.
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Investigating the crystal structures of alkali and alkaline-earth metal salts of 2,5-(dianilino)terephthalic acid

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01501A, Paper
Eric Quarez, Elise Deunf, Vincent Cadiou, Thibaut Gutel, Florent Boucher, Dominique Guyomard, Franck Dolhem, Philippe Poizot
Li, Na and Mg salts of 2,5-(dianilino)terephthalate exhibit systematically an original double layered structure composed of polar and non-polar slabs.
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Growth and characterization of all-inorganic lead halide perovskite semiconductor CsPbBr3 single crystals

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01709J, Paper
Mingzhi Zhang, Zhiping Zheng, Qiuyun Fu, Zheng Chen, Jianle He, Sen Zhang, Liang Yan, Yunxiang Hu, Wei Luo
The crystal structure transforms from orthorhombic to tetragonal at 88 [degree]C and then to cubic at 130 [degree]C.
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Single-crystal-to-single-crystal conversions of two metal-mediated photoreactive coordination polymers based on stereoselective [2 + 2] photocycloaddition reactions

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01402C, Paper
Jing-Min Chen, Qian-Kun Zhou, Yi-Xuan Hou, Dong Liu
Two stereoselective [2 + 2] photocycloaddition reactions occur in two metal-mediated coordination polymers via single-crystal-to-single-crystal transformations.
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New complexes constructed from in situ nitration of (1H-tetrazol-5-yl)phenol: synthesis, structures and properties

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE00753A, Paper
Ceng-Ceng Du, Xin-Fang Wang, Sheng-Bin Zhou, Duo-Zhi Wang, Dianzeng Jia
New complexes based on three precursors via in situ nitration have been prepared. Moreover, the solid state UV-vis spectra and band gap energy of those complexes were investigated, and the luminescent properties (1-3, 7 and 8) and magnetic properties (3-6 and 9) were also discussed.
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Synthesis, structure and optoelectronic properties of rigid 3D tetraindeno-fused spirofluorene with thioxanthene or dioxothioxanthene substitutes

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01407D, Paper
Jing Guan, Fangyuan Zhang, Yijiao Zhang, Zhigang Liu, Yanli Wu, Debin Xia
This work reports the synthesis and characterization of two blue emitters. Their 3D rigid structures are the appealing feature.
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Effects of crystalline growth on structural and luminescence properties of Ca(10-3x)Eu2x(PO4)6F2 nanoparticles fabricated by using a microwave driven hydrothermal process

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CrystEngComm, 2017, Advance Article
DOI: 10.1039/C7CE01454F, Paper
Katarzyna Zawisza, Paulina Sobierajska, Guillaume Renaudin, Jean-Marie Nedelec, Rafal J. Wiglusz
The structural and luminescence properties of Eu3+ doped nanofluorapatites obtained by hydrothermal method were investigated.
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